Schütte, SteffenSteffenSchüttePieper, UrsulaUrsulaPieperKlingebiel, UweUweKlingebielStalke, DietmarDietmarStalke2019-07-102019-07-101993https://resolver.sub.uni-goettingen.de/purl?gro-2/61013It was possible by crystallizing the lithiated derivative of di-tert-butylfluorosilanol to isolate a stable aquo-complex of this tetrameric compound as the first hydrolysis product. An X-ray diffraction study has revealed the existence of ([R2Si(F)OLi]3·[R2Si(OH)OLi] ·THF·H2O (R = CMe3; THF = tetrahydrofuran). The mechanism of hydrolysis from [R2Si(F)OLi]4 to this aquo-complex is discussed.application/pdfenGoescholarhttps://goescholar.uni-goettingen.de/licenseanorganische Chemie540journal_articlehttps://resolver.sub.uni-goettingen.de/purl?goescholar/3366openAccess