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Efficient synthesis of ortho-carborane by reaction of propiolic acid tert-butyl ester with decaborane(14)

dc.bibliographiccitation.firstpage1109
dc.bibliographiccitation.issue7
dc.bibliographiccitation.journalSynlett
dc.bibliographiccitation.lastpage1110
dc.contributor.authorTietze, Lutz Friedjan
dc.contributor.authorGriesbach, U.
dc.contributor.authorElsner, O.
dc.date.accessioned2018-11-07T10:24:14Z
dc.date.available2018-11-07T10:24:14Z
dc.date.issued2002
dc.description.abstractReaction of propiolic acid tert-butyl ester I and decaborane(14) at 90 degreesC did not give the expected carborane carboxylic acid tert-butyl ester 3 but directly unsubstituted ortho-carborane 2 which was isolated in 52% yield as pure material, An in situ de-tert-butoxycarbonylation of the first formed carborane carboxylic acid tert-butyl ester 3 via a six membered transition state is suggested for this domino process.
dc.identifier.isi000176746900017
dc.identifier.urihttps://resolver.sub.uni-goettingen.de/purl?gro-2/42618
dc.notes.statuszu prüfen
dc.notes.submitterNajko
dc.publisherGeorg Thieme Verlag Kg
dc.relation.issn0936-5214
dc.titleEfficient synthesis of ortho-carborane by reaction of propiolic acid tert-butyl ester with decaborane(14)
dc.typejournal_article
dc.type.internalPublicationyes
dc.type.peerReviewedyes
dc.type.statuspublished
dspace.entity.typePublication

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